Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 2-Methylbicyclo(2.2.1)heptan-2-ol | HCID 296920 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 572634 | HCID 572634 | — |
Reaction Steps
1 ml of 75% sulfuric acid was added to 240.0 g (1.9M) of the alcohol (II) obtained in 1--1) above and 500 ml of glacial acetic acid and the resulting mixture was stirred at 60° C. for three hours. After cooling, the reaction mixture was diluted with 3 l of water and then neutralized with sodium carbonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05463118 |
|---|
| Source dataset | uspto-grants-1995_10 |
|---|
| ORD ID | ord-c74bf94504904731bfa5875474d495e7 |
|---|
| Source note | uspto-grants-1995_10 |
|---|
