HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pivalic acid → 3-(Benzyloxy)-2,2-dimethylpropanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pivalic acid | HCID 6417 | — |
| Reactant | Methyl Oleate | HCID 5364509 | — |
| Product | 3-(Benzyloxy)-2,2-dimethylpropanoic acid | HCID 13478288 | — |
Reaction Steps
The spectroscopic data of the compound have already been reported further back in the text. Nafion SAC 13 was used as catalyst for acyloxylating methyl oleate. The following reaction conditions were selected: catalyst velocity 4 mmol/g of catalyst, molar excess of pivalic acid compared to methyl oleate=25, temperature 120° C., batch reaction under atmospheric pressure, reaction time 24 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07101831B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-f74b4594fba64171bc1542a310193146 |
| Source note | uspto-grants-2006_09 |