HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → Ethyl 3-(4-methylphenyl)-3-oxopropanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Ethyl 3-(4-chlorophenyl)-3-oxopropanoate | HCID 101336 | — |
| Reactant | HCID 21962140 | HCID 21962140 | — |
| Reactant | HCID 178485201 | HCID 178485201 | — |
| Product | Ethyl 3-(4-methylphenyl)-3-oxopropanoate | HCID 292637 | — |
Reaction Steps
The title compound was prepared from ethyl(4-chloro)benzoylacetate (5.0 g, 22 mmol) (obtained in preparation 2) and methylthiopseudourea.H2SO4 (3.31 g, 12 mmol) by following the procedure described in preparation 4, (0.573 g, 11.6%). MS m/z: 223 (M+). Preparation 6 Synthesis of 2-amino-6-(4-methylsulfanyl-phenyl)-1,3-oxazin-4-one
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07101873B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-78979f26236a4b67aa5edcd1ca3d81bb |
| Source note | uspto-grants-2006_09 |