Lawesson's reagent → HCID 10310225, compound

Participants

Reaction Steps

The product of Example 9 (0.40 g, 0.956 mmol) and Lawesson's reagent (0.290 g, 0.717 mmol) in dioxane (5 ml) are heated at 80° C. overnight. The reaction mixture is evaporated to dryness and the residue purified by PTLC (10% MeOH/DCM) to give the title compound as solid. Rf (10% MeOH/DCM)=0.66.

Provenance & Evidence