HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86760229, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86595393 | HCID 86595393 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 86760229 | HCID 86760229 | — |
Reaction Steps
(3R)-4-[(3R)-3-[(tert-Butoxycarbonyl)amino]-4-(2,4,5-trifluorophenyl)butanoyl]hexahydro-3-[4-(trifluoromethoxy)benzyl]-2H-1,4-diazepin-2-one was dissolved in 4M hydrogen chloride in dioxane and evaporated after 2.5 h to yield the desired product. LC/MS 504.2 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07101871B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-c59dbbe93086417e88139df386c4d13e |
| Source note | uspto-grants-2006_09 |