HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → N-[4-(2-Chloro-ethyl)-2-methyl-phenyl]-N-ethyl-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | N-[4-(2-Chloro-ethyl)-2-methyl-phenyl]-acetamide | HCID 21963464 | — |
| Product | N-[4-(2-Chloro-ethyl)-2-methyl-phenyl]-N-ethyl-acetamide | HCID 21963286 | 88% |
Reaction Steps
N-[4-(2-Chloro-ethyl)-2-methyl-phenyl]-N-ethyl-acetamide was prepared according to the general method as outlined in Preparation 43 starting from N-[4-(2-chloro-ethyl)-2-methyl-phenyl]-acetamide (0.40 g, 1.89 mmol) and ethyliodide (0.189 mL, 2.36 mmol). After chromatographic purification, the product was isolated as a viscous oil (0.399 g, 1.66 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07101886B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-61552842dc6841bd88d5f08d25dfbdea |
| Source note | uspto-grants-2006_09 |