反应详情

A solution of cyclopropyl phenyl sulfide (10.5 g, 70 mmol) and Oxone™ (55.13 g, 175 mmol) in methanol (30 ml) was stirred at room temperature for 5 hours. The mixture was diluted was water and extracted with ethyl acetate. The combined organic layers were dried (MgSO4) and concentrated in vacuo.

1. additionThe mixture was diluted
2. extractionextracted with ethyl acetate
3. dry with materialThe combined organic layers were dried (MgSO4)
4. concentrationconcentrated in vacuo