HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → Cyclopropanesulphonylbenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Benzene, (cyclopropylthio)- | HCID 123348 | — |
| Reactant | Potassium hydroxy sulfite | HCID 23707502 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Cyclopropanesulphonylbenzene | HCID 11309899 | — |
Reaction Steps
A solution of cyclopropyl phenyl sulfide (10.5 g, 70 mmol) and Oxone™ (55.13 g, 175 mmol) in methanol (30 ml) was stirred at room temperature for 5 hours. The mixture was diluted was water and extracted with ethyl acetate. The combined organic layers were dried (MgSO4) and concentrated in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07101892B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-cf85ed6b24364e7f880c4edaa04925ef |
| Source note | uspto-grants-2006_09 |