HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69583980, compound → HCID 21048984, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69583980 | HCID 69583980 | — |
| Catalyst | Rhodium | HCID 23948 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21048984 | HCID 21048984 | — |
Reaction Steps
Rhodium on carbon catalyst (15 mg) was added to a solution of the product from Example 145 (100 mg, 0.17 mmol) in methanol (30 mL) and the reaction hydrogenated at 30 psi for 4 hours. The mixture was then filtered through Celite® and evaporated to give an oil. (100 mg). MS (ES+) 579 ([MH]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07101895B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-932b6899445e4d278023b4098c93dcb2 |
| Source note | uspto-grants-2006_09 |