HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 13687902, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 69585034 | HCID 69585034 | — |
| Product | HCID 13687902 | HCID 13687902 | — |
Reaction Steps
Following the procedure for preparation of compound 119, and substituting bromophthalide with iodomethane, provided the title compound 120. 1H NMR (CD3OD, 400 MHz): 1.44 (s, 3H), 3.00 (dd, 2H), 3.80 (2 s, 6H), 4.77 (s, 3H), 6.71–6.86 (m, 3H). MS (ESI) m/z 269.33 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07101912B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-b0b30c9780484853a05c4e011cf5246f |
| Source note | uspto-grants-2006_09 |