Hydrochloric Acid → HCID 17978209, compound

Participants

Reaction Steps

15.08 g of N,N-dimethylcyclohexylamine and 700 ml of heptane were placed under argon in a 500 ml three-necked flask fitted with internal thermometer and gas inlet stopcock. HCl gas from a gas generation apparatus was passed into this reaction mixture for 1 hour. The N,N-dimethylcyclohexylammonium hydrochloride formed was separated off via a G4 frit, washed with 100 ml of heptane and dried in an oil pump vacuum. 19.0 g (98%) of the desired product were isolated.

Provenance & Evidence