Hydrochloric Acid → HCID 17978209, compound

HRID 2212457Notes

Reaction equation

HRID 2212457 reaction equation
[CH3:1][N:2]([CH:4]1[CH2:9][CH2:8][CH2:7][CH2:6][CH2:5]1)[CH3:3].[ClH:10]>CCCCCCC>[ClH:10].[CH3:1][NH+:2]([CH:4]1[CH2:9][CH2:8][CH2:7][CH2:6][CH2:5]1)[CH3:3]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 7415N,N-Dimethylcyclohexylamine

Product 1

HCID 17978209HCID 17978209, compound

Reagents, catalysts & solvents 1

HCID 8900HeptaneSolvent

Procedure

15.08 g of N,N-dimethylcyclohexylamine and 700 ml of heptane were placed under argon in a 500 ml three-necked flask fitted with internal thermometer and gas inlet stopcock. HCl gas from a gas generation apparatus was passed into this reaction mixture for 1 hour. The N,N-dimethylcyclohexylammonium hydrochloride formed was separated off via a G4 frit, washed with 100 ml of heptane and dried in an oil pump vacuum. 19.0 g (98%) of the desired product were isolated.

Workup

  1. customfitted with internal thermometer and gas inlet stopcock

Sources & evidence

ORD record
ord-789fd31a48cd42beac6ede5212952d9e
Source dataset
uspto-grants-2006_09
Patent number
US07101940B2

Reaction notes

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