Hydrochloric Acid → HCID 17978210, compound

HRID 2212459Notes

Reaction equation

HRID 2212459 reaction equation
[CH3:1][N:2]([CH:4]([CH3:6])C)[CH3:3].[ClH:7].[CH3:8][CH2:9][CH2:10][CH2:11][CH2:12]CC>>[ClH:7].[CH3:1][NH+:2]([CH2:4][C:6]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)[CH3:3]

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 8900HeptaneHCID 70452N,N-Dimethylisopropylamine

Product 1

HCID 17978210HCID 17978210, compound

Procedure

6 g of N,N-dimethylisopropylamine and 300 ml of heptane were placed under argon in a 500 ml three-necked flask fitted with internal thermometer and gas inlet stopcock. HCl gas from a gas generation apparatus was passed into this reaction mixture for 1 hour. The N,N-dimethylbenzylammonium hydrochloride formed was separated off via a G4 frit, washed with 100 ml of heptane and dried in an oil pump vacuum. 7.4 g (87%) of the desired product were isolated.

Workup

  1. customfitted with internal thermometer and gas inlet stopcock

Sources & evidence

ORD record
ord-01a518d5a7e9418f8b86a78642d989fa
Source dataset
uspto-grants-2006_09
Patent number
US07101940B2

Reaction notes

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