HCID 86602635, compound → HCID 90744006, compound

Participants

Reaction Steps

(1S,2S,4S)-4-(Benzyloxy)-2-(tert-butyldimethylsilyloxy)-N-((S)-1-phenylethyl)cyclohexanamine MS: 440 (M+H)+; HPLC Ret Time: 2.83 min (YMC Xterra S5 4.6×50 mm column, 3 min gradient, 4 mL/min) was obtained from (1S,2S,5S)-5-(benzyloxy)-2-((S)-1-phenylethylamino)-cyclohexanol) 39A as described in 39B. It was then converted to the product as described in 39B and exhibited an [a]25589 19.2 (c 5.7, MeOH).

Provenance & Evidence