HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → Malononitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 178509172 | HCID 178509172 | — |
| Product | Malononitrile | HCID 8010 | — |
| Product | 5-Aminoquinoline | HCID 11911 | — |
| Product | HCID 178509172 | HCID 178509172 | — |
Reaction Steps
In a manner similar to that described in Example 53, 4-(quinolin-5-ylhydrazono)-4H-pyrazole-3,5-diamine was prepared. 5-Aminoquinoline (0.35 g), malononitrile (0.3 g) and hydrazine hydrate (0.3 mL) yielded 0.043 g of the title compound after the purification by preparative TLC (⅓ of the crude product).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07105503B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-c079bced2bb948249f41560a60d00e52 |
| Source note | uspto-grants-2006_09 |