HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propenylguaiacol → HCID 69589350, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propenylguaiacol | HCID 7338 | — |
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69589350 | HCID 69589350 | — |
Reaction Steps
To manufacture this combination Epichlorohydrin was mixed with isoeugenol and NaOH dissolved in ethanol and boiled to reflux for 2–6 hours. Ethanol was then removed from the resulting mixture and the mixture was passed through silica gel column eluted with n-hexane and ethyl acetate, and dried with reduced pressure, to obtain 4-epoxy isoeugenol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07105521B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-73008e7bfd4246e0a4b7df7ffc23ced4 |
| Source note | uspto-grants-2006_09 |