HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 21955290, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | tert-Butyl 5,6-dihydroimidazo(1,2-a)pyrazine-7(8H)-carboxylate | HCID 21955306 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21955290 | HCID 21955290 | — |
Reaction Steps
1,1-Dimethylethyl 5,6,7,8-tetrahydroimidazo[1,2-a]pyrazin-7-carboxylate (Description 163, 505 mg, 2.26 mmol) in dichloromethane (2.5 mL) was added to stirred, cooled (0° C.) trifluoroacetic acid (5 mL) and the mixture was stirred at 0° C. for 15 minutes, then at room temperature for 45 minutes. The solvent was evaporated under reduced pressure to give the title compound. m/z (ES+) 124 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07105507B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-48b78878247741ff961ec000ecb7ef25 |
| Source note | uspto-grants-2006_09 |