HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21912551, compound → HCID 86760242, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21912551 | HCID 21912551 | — |
| Reactant | HCID 21955404 | HCID 21955404 | — |
| Product | HCID 86760242 | HCID 86760242 | — |
Reaction Steps
Preparation took place in analogy to I.B.23 by reacting [5-(2-methoxy-2-oxoethyl)-11-oxo-5,11-dihydro-10H-dibenzo[b,e]-[1,4]diazepin-10-yl]acetic acid 37c with N-[4-(aminomethyl)1,3-thiazol-2-yl]-N′-benzylurea (hydrochloride) (38). Chromatography on silica gel (CH2Cl2/CH3OH 2→10%) afforded 0.45 g; ESI-MS [M+H+]=585.25.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07105508B1 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-aef6bbb5cedd421592a4e8b402ffc77b |
| Source note | uspto-grants-2006_09 |