HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine-2-carbonitrile → Picolinimidohydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine-2-carbonitrile | HCID 7522 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Picolinimidohydrazide | HCID 70493 | — |
Reaction Steps
2-Cyanopyridine (5.2 g, 50 mmol) and hydrazine hydrate (2.95 g, 50 mmol) were mixed and a small amount of ethanol was added to obtain a clear solution. After standing overnight at ambient temperature, the resulting white crystals were collected by filtration. The resulting product was washed with diethyl ether and dried in the air to afford pyridine-2-carbohydrazonamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07105548B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-c839c168255a492e873e23d1f0d201dc |
| Source note | uspto-grants-2006_09 |