Methyl iodide → HCID 69633142, compound

Participants

Reaction Steps

Prepared from (2S)-3-(3,4-dichlorophenyl)-2-methyl-N-(7-chloro-2-oxo-5phenyl-2,3dihydro-1H-benzo[e][1,4]diazepin-3-yl)-propionamide by treatment with methyl iodide (c.f Step 2B, Scheme 2) (1H, CDCl3) 1.27 (3H, d, J=7 Hz), 2.68 (2H, m), 2.96 (1H, m), 3.43 (3H, s), 5.41 (1H, d, J=7.9 Hz), 7.05 (1H, m), 7.14 (1H, m), 7.32–7.36 (4H, m), 7.41 (2H, m), 7.48 (1H, m), 7.54–7.58 (3H, m); MS(CI+): MH+:516.

Provenance & Evidence