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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2213367Generated: October 30, 2026

1,2-Dichloroethane → HCID 21957345, compound

https://huagongshe.com/reaction/2213367

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,2-DichloroethaneHCID 11—
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 21051178HCID 21051178—
ProductHCID 21957345HCID 21957345—

Reaction Steps

1-[4-(5-Aminomethyl-2-oxo-oxazolidin-3-yl)-phenyl]-2,3-dihydro-1H-pyridin-4-one hydrochloride is prepared from {3-[4-(4-oxo-3,4-dihydro-2H-pyridin-1-yl)-phenyl]-2-oxo-oxazolidin-5-ylmethyl}-carbamic acid tert-butyl ester following the method described for Example 3 using 25% TFA in DCE. MS (m/z): 288 [M−HCl+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07105547B2
Source datasetuspto-grants-2006_09
ORD IDord-7cdc8b92fa5c4831ac15fd0e027c976f
Source noteuspto-grants-2006_09