HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dichloroethane → HCID 21957345, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dichloroethane | HCID 11 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 21051178 | HCID 21051178 | — |
| Product | HCID 21957345 | HCID 21957345 | — |
Reaction Steps
1-[4-(5-Aminomethyl-2-oxo-oxazolidin-3-yl)-phenyl]-2,3-dihydro-1H-pyridin-4-one hydrochloride is prepared from {3-[4-(4-oxo-3,4-dihydro-2H-pyridin-1-yl)-phenyl]-2-oxo-oxazolidin-5-ylmethyl}-carbamic acid tert-butyl ester following the method described for Example 3 using 25% TFA in DCE. MS (m/z): 288 [M−HCl+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07105547B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-7cdc8b92fa5c4831ac15fd0e027c976f |
| Source note | uspto-grants-2006_09 |