4-Methoxybenzaldehyde → HCID 21957905, compound

HRID 2213581Notes

Reaction equation

[CH3:1][O:2][C:3]1[CH:10]=[CH:9][C:6]([CH:7]=O)=[CH:5][CH:4]=1.[CH2:11]([C:19]1[CH:25]=[CH:24][C:22]([NH2:23])=[CH:21][CH:20]=1)[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]>>[CH3:1][O:2][C:3]1[CH:10]=[CH:9][C:6]([CH2:7][NH:23][C:22]2[CH:24]=[CH:25][C:19]([CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])=[CH:20][CH:21]=2)=[CH:5][CH:4]=1

Participants

Reactant 2

HCID 312444-Methoxybenzaldehyde

HCID 853464-Octylaniline

Product 1

HCID 21957905HCID 21957905, compoundYield 99.1%

Procedure

By the reaction and treatment in the same manner as in Preparation Example 1 using 4-methoxybenzaldehyde (1.0 g) and 4-octylaniline (1.4 g) as starting materials, [(4-methoxyphenyl)methyl](4-octylphenyl)amine (2.2 g) was obtained.

Workup

customBy the reaction and treatment in the same manner

Sources & evidence

ORD record: ord-f202ac8abfcd4c6ebf5729ce7c79679e
Source dataset: uspto-grants-2006_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07105567B2

Reaction notes

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