4-Isopropylaniline → HCID 21957910, compound

HRID 2213594Notes

Reaction equation

[CH:1]1[C:6]([CH:7]=O)=[CH:5][C:4]2[O:9][CH2:10][O:11][C:3]=2[CH:2]=1.[CH:12]([C:15]1[CH:21]=[CH:20][C:18]([NH2:19])=[CH:17][CH:16]=1)([CH3:14])[CH3:13]>>[O:11]1[C:3]2[CH:2]=[CH:1][C:6]([CH2:7][NH:19][C:18]3[CH:20]=[CH:21][C:15]([CH:12]([CH3:14])[CH3:13])=[CH:16][CH:17]=3)=[CH:5][C:4]=2[O:9][CH2:10]1

Participants

Reactant 2

HCID 74644-Isopropylaniline

HCID 8438Piperonal

Product 1

HCID 21957910HCID 21957910, compoundYield 76.6%

Procedure

By the reaction and treatment in the same manner as in Preparation Example 1 using piperonal (4.5 g) and 4-isopropylaniline (4.0 g) as starting materials, (benzo[d]1,3-dioxolen-5-ylmethyl)(4-isopropylphenyl)amine (6.1 g) was obtained.

Workup

customBy the reaction and treatment in the same manner

Sources & evidence

ORD record: ord-f5e54f6d80f64ae2a6353f15358c28ff
Source dataset: uspto-grants-2006_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07105567B2

Reaction notes

Loading…