HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Diisopropylphenyl isocyanate → N'-(2,6-diisopropylphenyl)-N-[(4-dimethylaminophenyl)methyl]-N-(4-trifluoromethylphenyl)urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Diisopropylphenyl isocyanate | HCID 92259 | — |
| Reactant | [(4-Dimethylaminophenyl)methyl](4-trifluoromethylphenyl)amine | HCID 21957911 | — |
| Product | N'-(2,6-diisopropylphenyl)-N-[(4-dimethylaminophenyl)methyl]-N-(4-trifluoromethylphenyl)urea | HCID 21957953 | 13.6% |
Reaction Steps
By the reaction and treatment in the same manner as in Example 1 using [(4-dimethylaminophenyl)methyl](4-trifluoromethylphenyl)amine (1.0 g) and 2,6-diisopropylphenyl isocyanate (0.83 g) as starting materials, N′-(2,6-diisopropylphenyl)-N-[(4-dimethylaminophenyl)methyl]-N-(4-trifluoromethylphenyl)urea (0.23 g) was obtained. melting point: 129–130° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07105567B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-05ccdf48101b4af1bd82ad7ed075923e |
| Source note | uspto-grants-2006_09 |