HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromopropane → HCID 66673967, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromopropane | HCID 7840 | — |
| Reactant | HCID 57954443 | HCID 57954443 | — |
| Catalyst | Tetrabutylammonium Iodide | HCID 67553 | — |
| Product | HCID 66673967 | HCID 66673967 | — |
Reaction Steps
cis-[3-(3-Pyridin-4-yl-[1,2,4]oxadiazol-5-yl)cyclopentyl]methanol (Preparation 5) was reacted with 1-bromopropane in the presence of tetrabutylammonium iodide, using a similar procedure to that described in Example 106, to afford the title compound: RT=3.69 min, m/z (ES+)=288.3 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08207147B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-bf257288622f49f589930e653a745181 |
| Source note | uspto-grants-2012_06 |