HRID221409

反应详情

EQUATION

反应方程式

HRID 221409 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

{3-[1-[tert-Butoxycarbonyl-(2-methoxy-ethyl)-amino]-2-(tert-butyl-dimethyl-silanyloxy)ethyl]-phenyl}-carbamic acid benzyl ester was added to ethanolic HCl (20 mL) at 0° C., allowed to warm to room temperature and stirred overnight. The reaction mixture was concentrated to give the title compound as a light yellow oil (300 mg).

WORKUP

后处理

  1. concentrationThe reaction mixture was concentrated