Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 2470061 | HCID 2470061 | — |
| Reactant | Sodium Nitrite | HCID 23668193 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178516905 | HCID 178516905 | — |
Reaction Steps
A solution of 11.04 g (160 mmol) of sodium nitrite in 40 ml of water was added to a solution of 12 g (39.3 mmol) of 4,5-dichloro-2-naphthalen-1-ylmethyl-2H-pyridazin-3-one in 120 ml of dimethylformamide and the mixture was stirred for 24 hours at 85° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07109192B2 |
|---|
| Source dataset | uspto-grants-2006_09 |
|---|
| ORD ID | ord-daabfef70cdd44a88ca1827ddfdeccca |
|---|
| Source note | uspto-grants-2006_09 |
|---|
