HuagongsheHuagongshe Chemistry Print Report · For research reference only
Indoline → HCID 20766004, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Indoline | HCID 10328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Methyl 3-bromopropanoate | HCID 76934 | — |
| Product | HCID 20766004 | HCID 20766004 | — |
Reaction Steps
A solution of indoline (6.15 g), methyl 3-bromopropionate (13 g), potassium carbonate (21 g) in 150 mL of acetonitrie was refluxed fro 16 h. The reaction mixture was concentrated, mixed with 300 mL of ether. The mixed reaction solution was filtered, concentrated down to afford compound UUA (8 g). MS: 206 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07109222B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-f2ec34b7b445413495b2cfb73538120c |
| Source note | uspto-grants-2006_09 |