HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11788638, compound → HCID 21055355, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11788638 | HCID 11788638 | — |
| Reactant | 2-Hydroxy-5-methylthiophenol | HCID 12306961 | — |
| Product | HCID 21055355 | HCID 21055355 | — |
Reaction Steps
The title compound (Ib) is prepared according to a reaction sequence identical to that employed for the synthesis of 3-(R)-amino-3,4-dihydro-2H-1,5-benzoxathiepine (Ia-1) but using, as starting material, 2-hydroxy-5-methylthiophenol (IVb) instead of 2-hydroxythiophenol. The title compound (Ib) is obtained in the form of a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07109234B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-f3f0d9c83f3149908bba3a0878dc450c |
| Source note | uspto-grants-2006_09 |