Sulfuryl chloride → HCID 86598000, compound

Participants

Reaction Steps

A solution of (45) (4.76 mmol) in CH2Cl2 at 0° C. was treated with sulfuryl chloride (1.1 mmol) under N2 for 10 min, then the reaction mixture was concentrated to dryness in vacuo to afford the crude chloroformate (46) in quantitative yield, which used in the next step without further purification. 1H NMR (CDCl3, 400 MHz): δ 1.00 (d, 6H), 1.20 (d, 9H), 2.143 (m, 1H), 6.54 (d, 1H).

Provenance & Evidence