HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21941232, compound → HCID 21941239, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21941232 | HCID 21941232 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21941239 | HCID 21941239 | — |
Reaction Steps
Methyl 4-acetamido-3-nitrophenylacetate (40 g, 0.159 mol)) was dissolved in methanol (400 ml) and hydrogenated at 5 bar over a 5% palladium on carbon catalyst. The catalyst was removed by filtration and the filtrate evaporated in vacuo to give methyl 4-acetamido-3-aminophenylacetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07112553B1 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-518b62b384f94e299a8bfbff546c9370 |
| Source note | uspto-grants-2006_09 |