2,6-Benzothiazolediamine → HCID 21057936, compound

HRID 2216324Notes

Reaction equation

HRID 2216324 reaction equation
[NH:1]([C:6]([O:8][C:9]([CH3:12])([CH3:11])[CH3:10])=[O:7])[CH2:2][C:3]([OH:5])=O.[S:13]1[C:17]2[CH:18]=[C:19]([NH2:22])[CH:20]=[CH:21][C:16]=2[N:15]=[C:14]1[NH2:23]>>[NH2:23][C:14]1[S:13][C:17]2[CH:18]=[C:19]([NH:22][C:3](=[O:5])[CH2:2][NH:1][C:6](=[O:7])[O:8][C:9]([CH3:12])([CH3:11])[CH3:10])[CH:20]=[CH:21][C:16]=2[N:15]=1

Participants

3

Reactant 2

HCID 215042,6-BenzothiazolediamineHCID 78288N-(tert-butoxycarbonyl)glycine

Product 1

HCID 21057936HCID 21057936, compoundYield 20%

Procedure

The title compound was prepared from Boc-Gly-OH and 1,3-benzothiazol-2,6-diamine according to the procedure of EXAMPLE 51. The product was obtained as a yellow solid.

Workup

  1. customThe product was obtained as a yellow solid

Sources & evidence

ORD record
ord-aa888bb2e0da403d83cdb73a019da75a
Source dataset
uspto-grants-2006_09
Patent number
US07112590B2

Reaction notes

Loading…