Pyridine → HCID 69042193, compound

HRID 221633Notes

Reaction equation

HRID 221633 reaction equation
[CH2:1]([C:3]1[CH:9]=[C:8]([OH:10])[CH:7]=[CH:6][C:4]=1[OH:5])[CH3:2].[C:11]12([C:21](Cl)=[O:22])[CH2:20][CH:15]3[CH2:16][CH:17]([CH2:19][CH:13]([CH2:14]3)[CH2:12]1)[CH2:18]2.N1C=CC=CC=1>C(Cl)Cl>[C:11]12([C:21]([O:10][C:8]3[CH:7]=[CH:6][C:4]([OH:5])=[C:3]([CH2:1][CH3:2])[CH:9]=3)=[O:22])[CH2:18][CH:17]3[CH2:16][CH:15]([CH2:14][CH:13]([CH2:19]3)[CH2:12]1)[CH2:20]2

Participants

5

Reactant 3

HCID 1049PyridineHCID 989151-Adamantanecarbonyl chlorideHCID 3083760Ethylhydroquinone

Product 1

HCID 69042193HCID 69042193, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

2-Ethylhydroquinone (1.85 mmol) and 1-adamantanecarbonyl chloride (1.4 eq.) were suspended in CH2Cl2 (3 mL/mmol), pyridine (1 mmol) was added, and the mixture stirred at r.t. for 48 h.

Sources & evidence

ORD record
ord-e88bde19e3db4c6c8fdc49e8c85b1e0e
Source dataset
uspto-grants-2012_06
Patent number
US08207174B2

Reaction notes

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