Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 2-Benzyl-6-methoxypyridine | HCID 21942274 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178515992 | HCID 178515992 | 70.9% |
Reaction Steps
A mixture of 59 g of 2-benzyl-6-methoxypyridine and 200 ml of 47% hydrobromic acid was heated under stirring in an oil bath at 100° C. for 7 hours. After standing to cool, 250 ml of water was added and the resulting crystals were filtered, washed with water and dried under reduced pressure, to give 38.9 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07112593B2 |
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| Source dataset | uspto-grants-2006_09 |
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| ORD ID | ord-8432c46a7bbf42feb057a7de3b73cea2 |
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| Source note | uspto-grants-2006_09 |
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