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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2216339Generated: October 25, 2026

Hydrogen Bromide → HCID 178515992, compound

https://huagongshe.com/reaction/2216339

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrogen BromideHCID 260—
Reactant2-Benzyl-6-methoxypyridineHCID 21942274—
SolventWaterHCID 962—
ProductHCID 178515992HCID 17851599270.9%

Reaction Conditions

Temperature100 °C

Reaction Steps

A mixture of 59 g of 2-benzyl-6-methoxypyridine and 200 ml of 47% hydrobromic acid was heated under stirring in an oil bath at 100° C. for 7 hours. After standing to cool, 250 ml of water was added and the resulting crystals were filtered, washed with water and dried under reduced pressure, to give 38.9 g of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07112593B2
Source datasetuspto-grants-2006_09
ORD IDord-8432c46a7bbf42feb057a7de3b73cea2
Source noteuspto-grants-2006_09