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HRID221634

反应详情

EQUATION

反应方程式

HRID 221634 的结构方程式

REACTANTS

反应物

2
结构：BrCC1CO1
HCID18430

Epibromohydrin

C3H5BrO

结构：CC(C)(C)[Si](C)(C)Oc1ccc(O)cc1
HCID597388

4-(tert-Butyldimethylsiloxy)phenol

C12H20O2Si

PRODUCTS

生成物

1
结构：CC(C)(C)[Si](C)(C)Oc1ccc(OCC2CO2)cc1
HCID19385012

未命名化合物

收率 21%

PROCEDURE

实验过程

Synthesis followed SP3a, using 4.1 mmol 4-(tert-Butyl-dimethyl-silanyloxy)-phenol and racemic epibromohydrine to give the title compound upon purification by Flash Master Personal (20 g silica gel cartridge, PE to PE/ethyl acetate 15:1) with 21% yield.

WORKUP

后处理

  1. customSynthesis