HCID 11384502, compound → HCID 11258624, compound

Participants

Reaction Steps

To a solution of methyl ester 2.3 (52 mg, 0.125 mmol) in benzene (5 ml), was added 10 mg of 10% Pd-C. The atmosphere was evacuated and flushed with H2 gas (3×), and the solution stirred for 1.5 h. The mixture was filtered and concentrated to give 52 mg (100%) of 6.1. MS (ESI) 419.4 (M+H+).

Provenance & Evidence