HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 58700790, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Boron Trichloride | HCID 25135 | — |
| Reactant | HCID 11351275 | HCID 11351275 | — |
| Product | HCID 58700790 | HCID 58700790 | 100.6% |
Reaction Steps
According to the procedure for preparation of 4.3, debenzylation of 10.1 (440 mg, 0.99 mmol) with 1M BCl3 in dichloromethane (4.95 ml, 4.95 mmol) yielded 353 mg (100%) of 10.3. MS (ESI) 355.4 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07112601B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-076d7981c8504120ba307af9c55fe8e0 |
| Source note | uspto-grants-2006_09 |