HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propylamine → HCID 21943416, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propylamine | HCID 7852 | — |
| Reactant | 2-(4-Methylphenyl)oxirane | HCID 108111 | — |
| Product | HCID 21943416 | HCID 21943416 | 49.6% |
Reaction Steps
4-Methyl styrene oxide(1.0 g,8.0 mmol)and 3 ml of propylamine in methanolic solution were charged into a flask. The flask was sealed and put in a refrigerator for 5–7 days. The solution was concentrated and the residue crystallized from ether, the title compound was obtained as white needle crystals, mp. 73.0–75.1 C, yield 49.6%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07112605B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-413e87f8e5924ce0a49c00cc5b24664d |
| Source note | uspto-grants-2006_09 |