HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropylamine → HCID 21943411, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Reactant | 4-Chlorostyrene oxide | HCID 197010 | — |
| Product | HCID 21943411 | HCID 21943411 | 54.5% |
Reaction Steps
4-Chloro styrene oxide (1.24 g, 8.0 mmol) and 3 ml of cyclopropylamine in methanolic solution were charged into a flask. The flask was sealed and put in a refrigerator for 5–7 days. The solution was concentrated and the residue crystallized from ether, the title compound was obtained as white needle crystals, mp. 100.2–102° C., yield 54.5%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07112605B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-e39f8eb7f8254aba99c6e82de44a3ebf |
| Source note | uspto-grants-2006_09 |