HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178513423, compound → HCID 9882073, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178513423 | HCID 178513423 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 9882073 | HCID 9882073 | 20.3% |
Reaction Steps
A solution of N-[(2,5,6-trifluorobenzoyl)oxy]pyridine-2-carboximidamide (50 mg, 0.169 mmol) in pyridine (0.3 mL) was heated at 115° C. for 17 hours. Standard work up, and silica gel chromatography, afforded 9.5 mg (20%) of 3-(2-pyridyl)-5-(2,5,6-trifluorophenyl)-1,2,4-oxadiazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07112595B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-c0234e9fd4e240e4a6d35792d472ef0a |
| Source note | uspto-grants-2006_09 |