HRID2217478

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6422

未命名化合物

结构：COC(=O)c1ccc(NC(=O)[C@H]2C[C@@H](OC)CN2C(=O)OC(C)(C)C)cc1

HCID68808041

未命名化合物

PRODUCTS

生成物

结构：COC(=O)c1ccc(NC(=O)[C@H]2C[C@@H](OC)CN2)cc1

HCID68815558

未命名化合物

收率 100.1%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Into a solution of 7 (12.5 g, 33.0 mmol) in anhydrous CH2Cl2 (70 mL) was added TFA (20 mL). The solution was stirred at RT overnight before concentrating under reduced pressure to give 8 (9.19 g, 100%).

WORKUP

后处理

concentrationbefore concentrating under reduced pressure