HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 86601542, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 68807323 | HCID 68807323 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86601542 | HCID 86601542 | 100% |
Reaction Steps
Into a solution of 6 (0.33 g, 0.647 mmol) in anhydrous CH2Cl2 (10 mL) was added TFA (2 mL). The solution was stirred at RT for 4 h before concentrating under reduced pressure to give 7 (0.19 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07407972B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-cef345d74d4c46728e278a798fc71de0 |
| Source note | uspto-grants-2008_08 |