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HRID2217809

反应详情

EQUATION

反应方程式

HRID 2217809 的结构方程式

REACTANTS

反应物

2
结构：C=CCN(CC)C(=O)OC(C)(C)C
HCID71365398

tert-Butyl ethyl(prop-2-en-1-yl)carbamate

C10H19NO2

结构：Cc1ccc2nc(Cl)ccc2c1NC(=O)CC1CCCCC1
HCID86013006

未命名化合物

PRODUCTS

生成物

1
结构：CCN(CCCc1ccc2c(NC(=O)CC3CCCCC3)c(C)ccc2n1)C(=O)OC(C)(C)C
HCID86609737

未命名化合物

收率 44%

PROCEDURE

实验过程

Prepared according to the method of example 1(b), using N-(2-chloro-6-methyl-5-quinolinyl)-cyclohexaneacetamide (Example 15 (a)) (400 mg) and ethyl(2-propenyl)-carbamic acid, 1,1-dimethylethyl ester (Example 15 (b)) (277 mg). Purification (SiO2, ethyl acetate:isohexane 20:80 as eluant) gave the sub-title compound (260 mg).

WORKUP

后处理

  1. customPrepared
  2. customPurification (SiO2, ethyl acetate:isohexane 20:80 as eluant)