HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl ethyl(prop-2-en-1-yl)carbamate → HCID 86609737, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl ethyl(prop-2-en-1-yl)carbamate | HCID 71365398 | — |
| Reactant | HCID 86013006 | HCID 86013006 | — |
| Product | HCID 86609737 | HCID 86609737 | 44% |
Reaction Steps
Prepared according to the method of example 1(b), using N-(2-chloro-6-methyl-5-quinolinyl)-cyclohexaneacetamide (Example 15 (a)) (400 mg) and ethyl(2-propenyl)-carbamic acid, 1,1-dimethylethyl ester (Example 15 (b)) (277 mg). Purification (SiO2, ethyl acetate:isohexane 20:80 as eluant) gave the sub-title compound (260 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07408065B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-76664c7494f440daa958a8a906ebfa14 |
| Source note | uspto-grants-2008_08 |