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HRID2217810

反应详情

EQUATION

反应方程式

HRID 2217810 的结构方程式

REACTANTS

反应物

2
结构：C=CCN(CC)C(=O)OC(C)(C)C
HCID71365398

tert-Butyl ethyl(prop-2-en-1-yl)carbamate

C10H19NO2

结构：O=C(CC1CCCCC1)Nc1c(Cl)ccc2nc(Cl)ccc12
HCID86012996

未命名化合物

PRODUCTS

生成物

1
结构：CCNCCCc1ccc2c(NC(=O)CC3CCCCC3)c(Cl)ccc2n1.Cl.Cl
HCID11442565

未命名化合物

收率 57.1%

PROCEDURE

实验过程

Prepared according to the method of example 15, using N-(2,6-dichloro-5-quinolinyl)-cyclohexaneacetamide (Example 1(a)) (500 mg) and ethyl(2-propenyl)carbamic acid 1,1-dimethylethyl ester (330 mg). Recrystallisation (methanol/ethyl acetate) afforded the title compound as a solid (195 mg).

WORKUP

后处理

  1. customPrepared
  2. customRecrystallisation (methanol/ethyl acetate)