HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl ethyl(prop-2-en-1-yl)carbamate → HCID 11442565, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl ethyl(prop-2-en-1-yl)carbamate | HCID 71365398 | — |
| Reactant | N-(2,6-Dichloro-5-quinolinyl)-cyclohexaneacetamide | HCID 86012996 | — |
| Product | HCID 11442565 | HCID 11442565 | 57.1% |
Reaction Steps
Prepared according to the method of example 15, using N-(2,6-dichloro-5-quinolinyl)-cyclohexaneacetamide (Example 1(a)) (500 mg) and ethyl(2-propenyl)carbamic acid 1,1-dimethylethyl ester (330 mg). Recrystallisation (methanol/ethyl acetate) afforded the title compound as a solid (195 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07408065B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-846ea24a190a4217b6503abb8a35453e |
| Source note | uspto-grants-2008_08 |