HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Aminoquinoline → HCID 59768622, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Aminoquinoline | HCID 11911 | — |
| Reactant | 2-(1-Methylcyclohexyl)acetic acid | HCID 13697885 | — |
| Product | HCID 59768622 | HCID 59768622 | 17.8% |
Reaction Steps
Prepared according to the method of example 18, using 5-quinolinamine (230 mg) and 1-methyl-cyclohexaneacetic acid (250 mg). Purification (SiO2, methanol:dichloromethane 1:9 as eluant) followed by recrystallisation from methanol/ethyl acetate gave the title compound as a colourless solid (80 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07408065B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-7a1c2afd8ea74b80b3c13d9496684e3a |
| Source note | uspto-grants-2008_08 |