HRID2217814
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
Prepared according to the method of example 18, using 5-quinolinamine (250 mg) and cyclopentanepropanoic acid (270 mg). Purification (HPLC, Symmetry—0.1% aqueous trifluoroacetic acid/acetonitrile) followed by recrystallisation from methanol/ethyl acetate gave the title compound as a colourless solid (112 mg).
WORKUP
后处理
- customPrepared
- customPurification (HPLC, Symmetry—0.1% aqueous trifluoroacetic acid/acetonitrile)
- customfollowed by recrystallisation from methanol/ethyl acetate