HRID2217815
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
Prepared according to the method of example 1(b)/(c), using N-(2,6-dichloro-5-quinolinyl)-cyclohexaneacetamide (Example 1(a)) (130 mg) and [3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]propyl]-2-propenyl-carbamic acid, 1,1-dimethylethyl ester (example 22(a)) (152 mg). Purification (SiO2, methanol:dichloromethane 1:9 as eluant) gave the title compound as a colourless solid (21 mg).
WORKUP
后处理
- customPrepared
- customPurification (SiO2, methanol:dichloromethane 1:9 as eluant)