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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2217819Generated: October 27, 2026

1-Phenylcyclopropanecarboxylic acid → 1-Cyclohexylcyclopropane-1-carboxylic acid

https://huagongshe.com/reaction/2217819

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Phenylcyclopropanecarboxylic acidHCID 80206—
ReactantHCID 178418361HCID 178418361—
CatalystAdams' catalystHCID 345198—
SolventAcetic AcidHCID 176—
SolventEthanolHCID 702—
Product1-Cyclohexylcyclopropane-1-carboxylic acidHCID 5374502357.8%

Reaction Steps

To 1-phenyl-cyclopropanecarboxylic acid (0.500 g) in acetic acid (2 mL) was added Adams catalyst (0.050 g) in ethanol (0.3 mL). The reaction was left to stir for 48 hours under 5 bar of hydrogen. The reaction was filtered, washing with ethanol (10 mL) and water (10 mL). The resulting solid was collected by filtration and subsequently washed with water (10 mL) to afford the sub-titled compound (0.3 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07408065B2
Source datasetuspto-grants-2008_08
ORD IDord-5f11a481afb645a6a92f3fb09c7e6df5
Source noteuspto-grants-2008_08